logo-polimi
Loading...
Risorse bibliografiche
Risorsa bibliografica obbligatoria
Risorsa bibliografica facoltativa
Scheda Riassuntiva
Anno Accademico 2021/2022
Scuola Scuola di Ingegneria Industriale e dell'Informazione
Insegnamento 097746 - INDUSTRIAL HETEROGENEOUS CATALYSIS
  • 097743 - PREPARATION AND CHARACTERIZATION OF CATALYTIC MATERIALS
Docente Castoldi Lidia
Cfu 5.00 Tipo insegnamento Modulo Di Corso Strutturato

Corso di Studi Codice Piano di Studio preventivamente approvato Da (compreso) A (escluso) Insegnamento
Ing Ind - Inf (1 liv.)(ord. 270) - MI (347) INGEGNERIA CHIMICA*AZZZZ097746 - INDUSTRIAL HETEROGENEOUS CATALYSIS
Ing Ind - Inf (Mag.)(ord. 270) - MI (472) CHEMICAL ENGINEERING - INGEGNERIA CHIMICA*AZZZZ097746 - INDUSTRIAL HETEROGENEOUS CATALYSIS

Obiettivi dell'insegnamento

The aim of course is to provide skills and knowledge for the comprehension and quali-quantitative analysis of catalytic processes used in the industrial chemistry, environmental protection, energetic field and others. In particular, after a general introduction on the industrial heterogeneous catalysis and catalysts, this part of the course will deal with the preparation and characterization of catalytic materials. 

To promote teaching internationalization and to offer students the opportunity of different teaching methods, collaborative class will be activated involving prof. Edd Anders Blekkan from Norwegian University of Science and Technology (NTNU). With this proposal, PoliMi students should attend NTNU seminars for at least 1 CFU.

  •  

Risultati di apprendimento attesi

At the end of this part of course the students should:

Understand and apply core principles and concepts in heterogeneous catalysis.

Know the most important catalytic materials, and describe their functions.

Identify all the steps in the preparation method of a catalytic materials, related to specific cheractistics in the final product.

Plan and choose methods for characterization of key properties of catalytic materials.


Argomenti trattati

The modules are given as lectures, seminars, excercises, laboratory activities, self-study.

 

Industrial catalysis: introduction to historical data on industrial catalytic processes, relevance of today's industrial catalysis and catalyst market, stages involved in the development of a catalytic process, perspectives and future developments of catalysis.

General characteristics of heterogeneous catalysts: role of a catalyst in a chemical reaction, properties of industrial catalysts, homogeneous and heterogeneous catalysis, components of heterogeneous catalysts, crystal structures of heterogeneous catalysts.

Catalyst preparation: general overview of the preparation method for bulk catalysts and supports. Theory and practice of (co)-precipitaion, impregnation, sol-gel methods, and of other preparation methods. Unit operation (i.e. filtration drying, calcination...) for the preparation of heterogeneous catalysts will be considered.

Chemico-physical characterization of catalysts: General aspects on the characterization of bulk and supported catalysts. Morphological characterization: specific surface area and pore distribution. Adsorption techniques for the catalyst characterization: physical and chemical adsorption, models for adsorption isotherms, experimental techniques for the adsorption study. Spectroscopic and thermal techniques for the catalyst characterization: FTIR, Laser-Raman, UV-Vis, TG-DTA, DSC, XRD, EPR, SEM, TEM, ecc.. Chemical characterization: TPD, TPO, TPR, TPSR, ecc..


Prerequisiti

No pre-requisites are required


Modalità di valutazione

The final exam will be an orale and it must allow the student to:

• demonstrate that he has acquired a correct approach to the catalyst preparation methods

be able to choose the best preparation method related to the characteristic in the final catalyst

apply methods and tools to correctly characterize the catalytic materials


Bibliografia
Risorsa bibliografica facoltativaI. Chorkendorff, J.W. Niemantsverdriet, Concepts of modern catalysis and kinetics, Editore: Wiley-VCH, Anno edizione: 2007, ISBN: 987-3-527-31672-4
Risorsa bibliografica facoltativaJ.W. Niemantsverdriet, Spectroscopy in catalysis, Editore: Wiley-VCH, Anno edizione: 2007, ISBN: 978-3-527-31651-9

Software utilizzato
Software Info e download Virtual desktop
Ambiente virtuale fruibile dal proprio portatile dove vengono messi a disposizione i software specifici per all¿attività didattica
PC studente
Indica se è possibile l'installazione su PC personale dello studente
Aule
Verifica se questo software è disponibile in aula informatizzata
Altri corsi
Verifica se questo software è utilizzato in altri corsi
ORIGINLAB Origin Pro - SI NO

Forme didattiche
Tipo Forma Didattica Ore di attività svolte in aula
(hh:mm)
Ore di studio autonome
(hh:mm)
Lezione
32:30
48:45
Esercitazione
0:00
0:00
Laboratorio Informatico
0:00
0:00
Laboratorio Sperimentale
17:30
26:15
Laboratorio Di Progetto
0:00
0:00
Totale 50:00 75:00

Informazioni in lingua inglese a supporto dell'internazionalizzazione
Insegnamento erogato in lingua Inglese
Disponibilità di materiale didattico/slides in lingua inglese
Disponibilità di libri di testo/bibliografia in lingua inglese
Possibilità di sostenere l'esame in lingua inglese
schedaincarico v. 1.7.2 / 1.7.2
Area Servizi ICT
05/07/2022