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Dettaglio Insegnamento

Contesto
Anno Accademico 2021/2022
Corso di Studi Dott. - MI (1374) Chimica Industriale e Ingegneria Chimica / Industrial Chemistry and Chemical Engineering
Anno di Corso 1

Scheda Insegnamento
Codice Identificativo 050686
Denominazione Insegnamento ADVANCED ANALYTICAL METHODS AND DATA ANALYSIS
Tipo Insegnamento MONODISCIPLINARE
Crediti Formativi Universitari (CFU) 5.0
Programma sintetico NMR Spectroscopy: Nuclear spin orientation in a magnetic field. Quantum chemical description. Screening constants and spin-spin couplings. First order spectra and second order effects. Heteronuclear coupling. Fourier Transform NMR. Experimental set-up: locking and shimming. Main NMR parameters and their relationships. Spectra acquisition, data processing, apodization, main artifacts related to signal digitization. Basics of spectral interpretation. Selected exempla. Basic concepts of 2D NMR. Correlation based on chemical connectivity or dipolar interactions. Measurement of diffusivity by NMR spectroscopy. NMR of heterogeneous samples or soft matter: high resolution magic angle spinning NMR. Case study of small molecules entrapped in polymeric frames. Exercises: Tutorials on spectral interpretation in one and two dimensions. Tutorial on signal processing. Laboratory: Full set-up, data acquisition, data processing and faq on one of the NMR spectrometers of the Department. Recommended textbooks Course slides J. Keeler "Undersatanding NMR Spectroscopy", 2nd ed. Wiley Exam: written test
Settori Scientifico Disciplinari (SSD) --

Dettaglio
Scaglione Docente Programma dettagliato
Da (compreso) A (escluso)
A ZZZZ Castiglione Franca, Mele Andrea --
manifestidott v. 1.7.0 / 1.7.0
Area Servizi ICT
12/08/2022